DEFAR - Artigos publicados em periódicos
URI permanente para esta coleçãohttp://www.hml.repositorio.ufop.br/handle/123456789/531
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Resultados da Pesquisa
Item Potencial fitotóxico de Pterodon polygalaeflorus Benth (Leguminosae) sobre Acanthospermum australe (Loefl.) O. Kuntze e Senna occidentalis (L.).(2009) Belinelo, Valdenir José; Vieira Filho, Sidney Augusto; Almeida, Marcelo Suzart de; Alves, Dalton Luiz FerreiraO objetivo dessa pesquisa foi sintetizar e caracterizar a atividade alelopática de derivados do ácido 6α,7β–di-hidroxivouacapan-17β–óico, isolado de sementes de Pterodon polygalaeflorus Benth (Leguminosae). A caracterização dos compostos envolveu espectrometria no infravermelho (IV) e ressonância magnética nuclear de hidrogênio e de carbono (RMN de 1H e de 13C) incluindo experimentos em duas dimensões (COSY 1H 1H, HMQC e HMBC). Os efeitos alelopáticos foram avaliados através de bioensaios de germinação de sementes e crescimento radicular, em condições controladas de temperatura (25 °C) e fotoperíodo (12 h claro/12h escuro), durante 72 horas. Concentrações de 1,0, 100,0 e 1000,0 mg.L-1 foram testadas. Senna occidentalis (fedegoso) e Acanthospermum australe (carrapichinho) foram utilizadas como espécies daninhas alvo. Foi observado que o efeito alelopático dos compostos aumentou em função do aumento da concentração, mostrando assim uma relação dose dependente. A tendência geral observada nos resultados foi de aumento da intensidade dos efeitos alelopáticos inibitórios em função do aumento da concentração. A N-Etil-6α-acetoxi-7β- hidroxivouacapan-17β–amida e N,N-Dietil-6α-acetoxi-7β-hidroxivouacapan-17β–amida foram os derivados que apresentaram maior efeito inibidor da germinação e do crescimento radicular do fedegoso e do carrapichinho. Portanto, esses compostos representam grande potencial aleloquimico contra essas ervas daninha.Item Samaras of Austroplenckia Populnea (Celastraceae) : new constituents and effect of extracts and friedelin on germination of Bidens Pilosa (Asteraceae).(2014) Caneschi, Carolina Milagres; Souza, Shiara Martins de; Certo, Thais Seixas; Souza, Gustavo Henrique Bianco de; Campos, Michele Soares Tacchi; Duarte, Lucienir Pains; Silva, Grácia Divina de Fátima; Gomes, Marcos de Souza; Vieira Filho, Sidney AugustoObjective: Evaluation of the impact of extracts and constituents from samaras of Austroplenckia populnea on percentage of seed germination (%SG), germination speed index (GSI), length of rootlets (LR), seedling length (SL), and on dry mass (DM) of Bidens pilosa L weed. Methods: The powder of samaras was extracted with organic solvents providing the hexane (SAPEH), chloroform (SAPEC), ethyl acetate (SAPEAE) and ethanol (SAPEE) extracts. The terpene 1 was isolated from SAPEH by means of column and thin layer chromatography and identified through NMR spectroscopy. Each extract and 1 were subjected to growth inhibition assays evaluating the following parameters: %SG, GSI, LR, SL and DM, with five repetitions. Results: The compounds Friedelin (1), 7-hydroxy-clerodan-3-en-16,15:18,20-diolide (2), 3,5,7,4'-tetrahydroxy-6-methoxy-8-prenylflavanone (3), tetradecanamide (4), and 4-hydroxy-1,6,15-acetyloxy-8,9-benzoyloxy-agarofurane (5) were isolated from hexane extract of samaras of A. populnea and identified by spectroscopic data. The compounds 2, 3 and 5 were not previously described as being chemical constituents from Celastraceae family. In addition, the novel compounds 3 and 5 were described here for the first time. Substantial effect on the germination of B. pilosa L. (picãopreto) was observed after treatment of seeds with nonpolar extracts from Samaras of A. populnea. Friedelin inhibited the seed germination in the tested concentrations showing toxic properties against picão-preto. Conclusion: The germination inhibition of seeds was higher using nonpolar extracts than polar extract. Friedelin inhibited the seed germination in the tested concentrations showing toxic properties against B. pilosa.Item Anti-trypanosomal activity of pentacyclic triterpenes isolated from Austroplenckia populnea (Celastraceae).(2002) Duarte, Lucienir Pains; Vieira Filho, Sidney Augusto; Silva, Grácia Divina de Fátima; Sousa, José Rego de; Pinto, Artur da SilveiraFour pentacyclic triterpenes isolated from Austroplenckia populnea and four compounds of known anti T. cruzi or anti-malarial activity were tested. Of those triterpenes tested 20_-hydroxy-tingenone showed high activity, epikatonic acid was less active, while populnilic and populninic acids were inactive against the trypanosome of the subgenus Schizotrypanum tested. Benzonidazole, nifurtimox, ketoconazole and primaquine presented a remarkable dose-dependent inhibitory effect reaching practically to a total growth inhibition of the parasite at the end of incubation time. The trypanosome tested appear to be a suitable model for preliminary screen for anti T. (S.) cruzi compounds.